On the interest of synchrotron X-ray imaging for the study of solidification in metallic alloys

Henri Nguyen-Thi; Luc Salvo; Ragnvald H. Mathiesen; Lars Arnberg; Bernard Billia; Michel Suery; Guillaume Reinhart

doi:10.1016/j.crhy.2011.11.010

Use of large scale facilities for research in metallurgy

On the interest of synchrotron X-ray imaging for the study of solidification in metallic alloys
[De lʼintérêt de lʼimagerie X synchrotron pour lʼétude de la solidification dʼalliages métalliques]

Henri Nguyen-Thi ^1,² ; Luc Salvo ³ ; Ragnvald H. Mathiesen ⁴ ; Lars Arnberg ⁵ ; Bernard Billia ^1,² ; Michel Suery ³ ; Guillaume Reinhart ^1,²

¹ Aix Marseille University, IM2NP, campus Saint-Jérôme, 13397 Marseille cedex 20, France
² CNRS, IM2NP, campus Saint-Jérôme, 13397 Marseille cedex 20, France
³ Université de Grenoble – CNRS, laboratoire SIMAP-GPM2, 101, rue de la physique, 38402 Saint-Martin dʼHères cedex, France
⁴ Department of Physics, NTNU, N-7491 Trondheim, Norway
⁵ Department of Materials Technology, NTNU, N-7491 Trondheim, Norway

Comptes Rendus. Physique, Use of large scale facilities for research in metallurgy / Utilisation des grands instruments pour la recherche en métallurgie , Volume 13 (2012) no. 3, pp. 237-245.

Résumé
Abstract

Les récents développements de sources synchrotron plus puissantes ont apporté une amélioration considérable des performances en imagerie X. Ceci sʼest traduit par une augmentation continue de lʼimpact scientifique des expériences effectuées avec une source synchrotron dans de nombreux domaines de recherche sur les matériaux, et en particulier lʼétude de la solidification. Il est bien établi que lʼimagerie X est une méthode de choix pour les études in situ et en temps réel de la formation des microstructures de solidification dans les alliages métalliques, avec des résolutions spatio-temporelles pertinentes. Dans cet article, nous présentons des résultats illustrant les capacités actuelles de lʼimagerie X synchrotron dans de ce domaine de recherche, chacun dʼentre eux utilisant des techniques différentes (radiographie, topographie et tomographie X). Ces résultats démontrent le fort potentiel de ces techniques dʼanalyse pour lʼinvestigation de phénomènes dynamiques en science des matériaux.

Recent developments of more powerful synchrotron sources have led to vast improvements in the performance of X-ray imaging. This is manifested by a continuous increase in the impact of synchrotron experiments in many research areas on materials, in particular solidification science. X-ray imaging has been established as a method of choice for in situ and real-time studies of solidification microstructure formation in metallic alloys, with spatio-temporal resolutions at the scales of relevance. In this article, we present illustrative results of the current capabilities of synchrotron X-ray imaging in this field of research, each of them using different X-ray techniques (radiography, topography and tomography). Those results demonstrate the high potential of these techniques for the investigation of dynamical phenomena in materials processing.

Publié le : 2012-01-28

DOI : 10.1016/j.crhy.2011.11.010

Keywords: Solidification, Synchrotron, Radiography, Topography, Tomography, Microstructure, Alloys
Mots-clés : Solidification, Synchrotron, Radiographie, Topographie, Tomographie, Microstructure, Alliages

Affiliations des auteurs :

Henri Nguyen-Thi ^{1, 2} ; Luc Salvo ³ ; Ragnvald H. Mathiesen ⁴ ; Lars Arnberg ⁵ ; Bernard Billia ^{1, 2} ; Michel Suery ³ ; Guillaume Reinhart ^{1, 2}

¹ Aix Marseille University, IM2NP, campus Saint-Jérôme, 13397 Marseille cedex 20, France
² CNRS, IM2NP, campus Saint-Jérôme, 13397 Marseille cedex 20, France
³ Université de Grenoble – CNRS, laboratoire SIMAP-GPM2, 101, rue de la physique, 38402 Saint-Martin dʼHères cedex, France
⁴ Department of Physics, NTNU, N-7491 Trondheim, Norway
⁵ Department of Materials Technology, NTNU, N-7491 Trondheim, Norway

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     title = {On the interest of synchrotron {X-ray} imaging for the study of solidification in metallic alloys},
     journal = {Comptes Rendus. Physique},
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Henri Nguyen-Thi; Luc Salvo; Ragnvald H. Mathiesen; Lars Arnberg; Bernard Billia; Michel Suery; Guillaume Reinhart. On the interest of synchrotron X-ray imaging for the study of solidification in metallic alloys. Comptes Rendus. Physique, Use of large scale facilities for research in metallurgy / 
Utilisation des grands instruments pour la recherche en métallurgie
, Volume 13 (2012) no. 3, pp. 237-245. doi : 10.1016/j.crhy.2011.11.010. https://comptes-rendus.academie-sciences.fr/physique/articles/10.1016/j.crhy.2011.11.010/

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Silvère Akamatsu; Henri Nguyen-Thi In situ observation of solidification patterns in diffusive conditions, Acta Materialia, Volume 108 (2016), p. 325 | DOI:10.1016/j.actamat.2016.01.024
L. Abou-Khalil; G. Salloum-Abou-Jaoude; G. Reinhart; C. Pickmann; G. Zimmermann; H. Nguyen-Thi Influence of gravity level on Columnar-to-Equiaxed Transition during directional solidification of Al – 20 wt. | DOI:10.1016/j.actamat.2016.03.007
Henri Nguyen-Thi; Guillaume Reinhart; Bernard Billia On the interest of microgravity experimentation for studying convective effects during the directional solidification of metal alloys, Comptes Rendus. Mécanique, Volume 345 (2016) no. 1, p. 66 | DOI:10.1016/j.crme.2016.10.007
Silvère Akamatsu; Mathis Plapp Eutectic and peritectic solidification patterns, Current Opinion in Solid State and Materials Science, Volume 20 (2016) no. 1, p. 46 | DOI:10.1016/j.cossms.2015.10.002
M Bedel; G Reinhart; A-A Bogno; H Nguyen-Thi; E Boller; Ch-A Gandin; H Henein Dendrite growth morphologies in rapidly solidified Al-4.5wt. | DOI:10.1088/1757-899x/117/1/012055
Sen Luo; Weiling Wang; Miaoyong Zhu Validation and Simulation of Cellular Automaton Model for Dendritic Growth during the Solidification of Fe–C Binary Alloy with Fluid Flow, ISIJ International, Volume 56 (2016) no. 4, p. 564 | DOI:10.2355/isijinternational.isijint-2015-573
A.G. Murphy; R.H. Mathiesen; Y. Houltz; J. Li; C. Lockowandt; K. Henriksson; N. Melville; D.J. Browne Direct observation of spatially isothermal equiaxed solidification of an Al–Cu alloy in microgravity on board the MASER 13 sounding rocket, Journal of Crystal Growth, Volume 454 (2016), p. 96 | DOI:10.1016/j.jcrysgro.2016.08.054
Honggang Zhong; Yunhu Zhang; Xiangru Chen; Congsen Wu; Zhiqiang Wei; Qijie Zhai In Situ Observation of Crystal Rain and Its Effect on Columnar to Equiaxed Transition, Metals, Volume 6 (2016) no. 11, p. 271 | DOI:10.3390/met6110271
L. Abou-Khalil; G. Salloum-Abou-Jaoude; G. Reinhart; C. Pickmann; G. Zimmermann; Y. Houltz; J. Li; O. Janson; H. Nguyen-Thi In Situ Investigation of the Effects of Gravity Level Variations on the Directional Solidification Microstructures During Parabolic Flights, TMS 2016 145th Annual Meeting Exhibition (2016), p. 43 | DOI:10.1007/978-3-319-48254-5_6
L. Abou-Khalil; G. Salloum-Abou-Jaoude; G. Reinhart; C. Pickmann; G. Zimmermann; Y. Houltz; J. Li; O. Janson; H. Nguyen-Thi In Situ Investigation of The Effects of Gravity Level Variations on The Directional Solidification Microstructures During Parabolic Flights, TMS 2016: 145thAnnual Meeting Exhibition: Supplemental Proceedings (2016), p. 43 | DOI:10.1002/9781119274896.ch6
M. Bedel; G. Reinhart; A.-A. Bogno; Ch.-A. Gandin; S. Jacomet; E. Boller; H. Nguyen-Thi; H. Henein Characterization of dendrite morphologies in rapidly solidified Al–4.5 wt. | DOI:10.1016/j.actamat.2015.02.007
A.G. Murphy; W.U. Mirihanage; D.J. Browne; R.H. Mathiesen Equiaxed dendritic solidification and grain refiner potency characterised through in situ X-radiography, Acta Materialia, Volume 95 (2015), p. 83 | DOI:10.1016/j.actamat.2015.04.060
Amy J. Clarke; Damien Tourret; Seth D. Imhoff; Paul J. Gibbs; Kamel Fezzaa; Jason C. Cooley; Wah‐Keat Lee; Alex Deriy; Brian M. Patterson; Pallas A. Papin; Kester D. Clarke; Robert D. Field; James L. Smith X‐ray Imaging and Controlled Solidification of Al‐Cu Alloys Toward Microstructures by Design, Advanced Engineering Materials, Volume 17 (2015) no. 4, p. 454 | DOI:10.1002/adem.201400469
Fenfen Yang; Fei Cao; Rengeng Li; Huijun Kang; Yanan Fu; Tiqiao Xiao; Tongmin Wang In Situ Study on the Evolution of Dendrite Morphology Affected by Electric Field in Sn‐Bi Alloy, Advances in the Science and Engineering of Casting Solidification (2015), p. 207 | DOI:10.1002/9781119093367.ch25
Fenfen Yang; Fei Cao; Rengeng Li; Huijun Kang; Yanan Fu; Tiqiao Xiao; Tongmin Wang In Situ Study on the Evolution of Dendrite Morphology Affected by Electric Field in Sn-Bi Alloy, Advances in the Science and Engineering of Casting Solidification (2015), p. 209 | DOI:10.1007/978-3-319-48117-3_25
Mohd Arif Anuar Mohd Salleh; A. Sugiyama; Hideyuki Yasuda; Stuart D. McDonald; Kazuhiro Nogita In Situ Soldering Process Technique by Synchrotron X-Ray Imaging, Applied Mechanics and Materials, Volume 754-755 (2015), p. 508 | DOI:10.4028/www.scientific.net/amm.754-755.508
N. Calonne; F. Flin; B. Lesaffre; A. Dufour; J. Roulle; P. Puglièse; A. Philip; F. Lahoucine; C. Geindreau; J.‐M. Panel; S. Rolland du Roscoat; P. Charrier CellDyM: A room temperature operating cryogenic cell for the dynamic monitoring of snow metamorphism by time‐lapse X‐ray microtomography, Geophysical Research Letters, Volume 42 (2015) no. 10, p. 3911 | DOI:10.1002/2015gl063541
M Bedel; G Reinhart; Ch-A Gandin; A-A Bogno; H Nguyen-Thi; H Henein Evolution of the dendritic morphology with the solidification velocity in rapidly solidified Al-4.5wt. | DOI:10.1088/1757-899x/84/1/012016
D Tourret; A Karma; A J Clarke; P J Gibbs; S D Imhoff Three-dimensional Dendritic Needle Network model with application to Al-Cu directional solidification experiments, IOP Conference Series: Materials Science and Engineering, Volume 84 (2015), p. 012082 | DOI:10.1088/1757-899x/84/1/012082
Mohsen Eshraghi; Bohumir Jelinek; Sergio D. Felicelli Large-Scale Three-Dimensional Simulation of Dendritic Solidification Using Lattice Boltzmann Method, JOM, Volume 67 (2015) no. 8, p. 1786 | DOI:10.1007/s11837-015-1446-0
G. Salloum-Abou-Jaoude; J. Wang; L. Abou-Khalil; G. Reinhart; Z. Ren; N. Mangelinck-Noel; X. Li; Y. Fautrelle; Henri Nguyen-Thi Motion of equiaxed grains during directional solidification under static magnetic field, Journal of Crystal Growth, Volume 417 (2015), p. 25 | DOI:10.1016/j.jcrysgro.2014.10.058
Jean-Yves Buffiere; José Baruchel Hard X-Ray Synchrotron Imaging Techniques and Applications, Synchrotron Radiation (2015), p. 389 | DOI:10.1007/978-3-642-55315-8_13
E. Liotti; A. Lui; R. Vincent; S. Kumar; Z. Guo; T. Connolley; I.P. Dolbnya; M. Hart; L. Arnberg; R.H. Mathiesen; P.S. Grant A synchrotron X-ray radiography study of dendrite fragmentation induced by a pulsed electromagnetic field in an Al–15Cu alloy, Acta Materialia, Volume 70 (2014), p. 228 | DOI:10.1016/j.actamat.2014.02.024
J. Wang; Y. Fautrelle; Z. M. Ren; H. Nguyen-Thi; G. Salloum Abou Jaoude; G. Reinhart; N. Mangelinck-Noël; X. Li; I. Kaldre Thermoelectric magnetic flows in melt during directional solidification, Applied Physics Letters, Volume 104 (2014) no. 12 | DOI:10.1063/1.4870099
Tomohiro Takaki Phase-field Modeling and Simulations of Dendrite Growth, ISIJ International, Volume 54 (2014) no. 2, p. 437 | DOI:10.2355/isijinternational.54.437
G. Reinhart; H. Nguyen-Thi; N. Mangelinck-Noël; J. Baruchel; B. Billia In Situ Investigation of Dendrite Deformation During Upward Solidification of Al-7wt. | DOI:10.1007/s11837-014-1030-z
Tongmin Wang; Fei Cao; Peng Zhou; Huijun Kang; Zongning Chen; Yanan Fu; Tiqiao Xiao; Wanxia Huang; Qingxi Yuan Study on diffusion behavior and microstructural evolution of Al/Cu bimetal interface by synchrotron X-ray radiography, Journal of Alloys and Compounds, Volume 616 (2014), p. 550 | DOI:10.1016/j.jallcom.2014.07.172
James A. Polyblank; Julian M. Allwood; Stephen R. Duncan Closed-loop control of product properties in metal forming: A review and prospectus, Journal of Materials Processing Technology, Volume 214 (2014) no. 11, p. 2333 | DOI:10.1016/j.jmatprotec.2014.04.014
Georges Salloum-Abou-Jaoude; Henri Nguyen-Thi; Guillaume Reinhart; Ragnvald H. Mathiesen; Gerhard Zimmermann; Daniela Voss Characterization of Motion of Dendrite Fragment by X-Ray Radiography on Earth and under Microgravity Environment, Materials Science Forum, Volume 790-791 (2014), p. 311 | DOI:10.4028/www.scientific.net/msf.790-791.311
Guillaume Reinhart; Henri Nguyen-Thi; Brice Sarpi; Aboul Aziz Bogno; Bernard Billia In Situ Investigation of Grain Migration by TGZM during Solidification in a Temperature Gradient, Materials Science Forum, Volume 790-791 (2014), p. 323 | DOI:10.4028/www.scientific.net/msf.790-791.323
Henri Nguyen-Thi; Jiang Wang; Georges Salloum-Abou-Jaoude; Guillaume Reinhart; Imants Kaldre; Nathalie Mangelinck; Zhong Ming Ren; Leonids Buligins; Andris Bojarevics; Yves Fautrelle; Olga Budenkova; Tamzin Lafford In Situ and Real-Time Analysis of TEM Forces Induced by a Permanent Magnetic Field during Solidification of Al-4wt | DOI:10.4028/www.scientific.net/msf.790-791.420
G. Reinhart; Ch.-A. Gandin; N. Mangelinck-Noël; H. Nguyen-Thi; J.-E. Spinelli; J. Baruchel; B. Billia Influence of natural convection during upward directional solidification: A comparison between in situ X-ray radiography and direct simulation of the grain structure, Acta Materialia, Volume 61 (2013) no. 13, p. 4765 | DOI:10.1016/j.actamat.2013.04.067
V.T. Witusiewicz; U. Hecht; S. Rex In-situ observation of eutectic growth in Al-based alloys by light microscopy, Journal of Crystal Growth, Volume 372 (2013), p. 57 | DOI:10.1016/j.jcrysgro.2013.02.033
H. Nguyen-Thi; G. Reinhart; G. Salloum Abou Jaoude; R.H. Mathiesen; G. Zimmermann; Y. Houltz; D. Voss; A. Verga; D.J. Browne; A.G. Murphy XRMON-GF: A novel facility for solidification of metallic alloys with in situ and time-resolved X-ray radiographic characterization in microgravity conditions, Journal of Crystal Growth, Volume 374 (2013), p. 23 | DOI:10.1016/j.jcrysgro.2013.03.032

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