[Imagerie au rayonnement synchrotron pour les études de croissance cristalline]
Les caractéristiques des installations modernes de rayonnement synchrotron (faisceaux de rayons X intenses et cohérents) ont amené à une augmentation notable des possibilités des techniques dʼimagerie, tant en ce qui concerne la résolution spatiale et temporelle que le contraste de phase et les images tridimensionelles. Ceci permet dʼobtenir des informations sur la croissance cristalline qui ne peuvent être obtenues autrement. Après une brève description de techniques dʼimagerie aux rayons X au synchrotron, nous donnons des exemples originaux qui illustrent les possibilités nouvelles pour les études de croissance cristalline : caractérisation de cristaux produits pour des applications, tels les tri-cristaux de glace que lʼon fait pousser pour des études de déformation mécanique, SiC, silicium monocristallin pour des cellules solaires photovoltaïques, des études in situ et en temps réel de la croissance de quasicristaux (AlPdMn), et la tomographie ultrarapide pour lʼétude de la croissance de dendrites dans des alliages métalliques.
The features associated with modern synchrotron radiation machines (intense and coherent beams) result in a substantial extension of X-ray imaging capabilities in terms of spatial and temporal resolution, phase contrast and 3D images. This allows crystal growth-related information to be obtained which is not available otherwise. After briefly describing the main synchrotron radiation based imaging techniques of interest, we give original examples illustrating the new capabilities for crystal growth: characterisation of crystals grown for applications, such as ice tri-crystals produced for mechanical deformation studies; SiC; crystalline silicon for solar photovoltaic cells; in situ and in real time studies of quasicrystal growth (AlPdMn); and ultrafast tomography for the study of the growth of dendrites in metallic alloys.
Mots-clés : Croissance cristalline, Rayonnement synchrotron, Image tridimensionelle
José Baruchel 1 ; Marco Di Michiel 1 ; Tamzin Lafford 1 ; Pierre Lhuissier 2 ; Jacques Meyssonnier 3 ; Henri Nguyen-Thi 4, 5 ; Armelle Philip 3 ; Petra Pernot 1 ; Luc Salvo 2 ; Mario Scheel 1
@article{CRPHYS_2013__14_2-3_208_0,
author = {Jos\'e Baruchel and Marco Di Michiel and Tamzin Lafford and Pierre Lhuissier and Jacques Meyssonnier and Henri Nguyen-Thi and Armelle Philip and Petra Pernot and Luc Salvo and Mario Scheel},
title = {Synchrotron {X-ray} imaging for crystal growth studies},
journal = {Comptes Rendus. Physique},
pages = {208--220},
publisher = {Elsevier},
volume = {14},
number = {2-3},
year = {2013},
doi = {10.1016/j.crhy.2012.10.010},
language = {en},
}
TY - JOUR AU - José Baruchel AU - Marco Di Michiel AU - Tamzin Lafford AU - Pierre Lhuissier AU - Jacques Meyssonnier AU - Henri Nguyen-Thi AU - Armelle Philip AU - Petra Pernot AU - Luc Salvo AU - Mario Scheel TI - Synchrotron X-ray imaging for crystal growth studies JO - Comptes Rendus. Physique PY - 2013 SP - 208 EP - 220 VL - 14 IS - 2-3 PB - Elsevier DO - 10.1016/j.crhy.2012.10.010 LA - en ID - CRPHYS_2013__14_2-3_208_0 ER -
%0 Journal Article %A José Baruchel %A Marco Di Michiel %A Tamzin Lafford %A Pierre Lhuissier %A Jacques Meyssonnier %A Henri Nguyen-Thi %A Armelle Philip %A Petra Pernot %A Luc Salvo %A Mario Scheel %T Synchrotron X-ray imaging for crystal growth studies %J Comptes Rendus. Physique %D 2013 %P 208-220 %V 14 %N 2-3 %I Elsevier %R 10.1016/j.crhy.2012.10.010 %G en %F CRPHYS_2013__14_2-3_208_0
José Baruchel; Marco Di Michiel; Tamzin Lafford; Pierre Lhuissier; Jacques Meyssonnier; Henri Nguyen-Thi; Armelle Philip; Petra Pernot; Luc Salvo; Mario Scheel. Synchrotron X-ray imaging for crystal growth studies. Comptes Rendus. Physique, Crystal growth / Croissance cristalline, Volume 14 (2013) no. 2-3, pp. 208-220. doi : 10.1016/j.crhy.2012.10.010. https://comptes-rendus.academie-sciences.fr/physique/articles/10.1016/j.crhy.2012.10.010/
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