<i>X</i>-ray line profiles analysis of plastically deformed metals

András Borbély; Tamás Ungár

doi:10.1016/j.crhy.2011.12.004

Use of large scale facilities for research in metallurgy

X-ray line profiles analysis of plastically deformed metals
[Profils de raie en rayons X sur des matériaux métalliques déformés plastiquement]

András Borbély ¹ ; Tamás Ungár ²

¹ SMS Materials Centre and CNRS UMR 5146, École des mines de Saint Etienne, 158, cours Fauriel, 42023 Saint Etienne, France
² Department of Materials Physics, Eötvös University Budapest, P.O. Box 32, Budapest H-1518, Hungary

Comptes Rendus. Physique, Use of large scale facilities for research in metallurgy / Utilisation des grands instruments pour la recherche en métallurgie , Volume 13 (2012) no. 3, pp. 293-306.

Résumé
Abstract

Nous présentons la base théorique de lʼanalyse des profils de raie en rayons X, et son application à la caractérisation microstructurale de métaux déformés plastiquement. La microstructure est décrite en termes de taille de domaine cohérent, densité de défauts planaires, densité de dislocations et un paramètre dʼarrangement des dislocations. Nous introduisons deux méthodes dʼanalyse : la méthode des moments, et la méthode étendue dʼajustement par analyse Convolutional Multiple Whole Profile. Nous présentons des exemples dʼutilisation de ces mesures sur la déformation plastique de monocristaux, de monocristaux résidant dans le volume dʼun polycristal, et dans le cas de familles de grains constituant des composantes de texture. Les exemples sélectionnés montrent le potentiel de la technique dʼanalyse du profil de raies obtenues soit par des sources de laboratoire ou par rayonnement synchrotron.

The theoretical basis of X-ray line profile analysis and its application to microstructural characterization of plastically deformed metallic alloys is presented. The microstructure is described in terms of coherent domain size, planar fault density, dislocation density and a dislocation arrangement parameter. Two evaluation methods are introduced: the momentum method and the extended Convolutional Multiple Whole Profile fit procedure. Their use is exemplified on plastically deformed single crystals, single grains residing in the bulk of a polycrystal and family of grains making up texture components. The selected examples show the potential of X-ray line profile analysis applied to diffraction patterns recorded with laboratory or synchrotron sources.

Publié le : 2012-01-28

DOI : 10.1016/j.crhy.2011.12.004

Keywords: Metals and alloys, X-ray diffraction, Line profile analysis, Dislocation density, Planar faults
Mots-clés : Métaux et alliages, Diffraction des rayons X, Analyse des profils de raie, Densité de dislocations, Défauts planaires

Affiliations des auteurs :

András Borbély ¹ ; Tamás Ungár ²

¹ SMS Materials Centre and CNRS UMR 5146, École des mines de Saint Etienne, 158, cours Fauriel, 42023 Saint Etienne, France
² Department of Materials Physics, Eötvös University Budapest, P.O. Box 32, Budapest H-1518, Hungary

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     title = {\protect\emph{X}-ray line profiles analysis of plastically deformed metals},
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András Borbély; Tamás Ungár. X-ray line profiles analysis of plastically deformed metals. Comptes Rendus. Physique, Use of large scale facilities for research in metallurgy / 
Utilisation des grands instruments pour la recherche en métallurgie
, Volume 13 (2012) no. 3, pp. 293-306. doi : 10.1016/j.crhy.2011.12.004. https://comptes-rendus.academie-sciences.fr/physique/articles/10.1016/j.crhy.2011.12.004/

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M. Nagaraj; B. Ravisankar WITHDRAWN: Investigation on microstructural properties of severe plastic deformed structural steel and evaluation of strengthening mechanisms, Materials Today Communications (2017) | DOI:10.1016/j.mtcomm.2017.12.006
Akira Taniyama; Toru Takayama; Masahiro Arai; Takanari Hamada Deformation Behavior of Cementite in Deformed High Carbon Steel Observed by X-ray Diffraction with Synchrotron Radiation, Metallurgical and Materials Transactions A, Volume 48 (2017) no. 10, p. 4821 | DOI:10.1007/s11661-017-4229-0
Vishtasb Soleimanian; Mohsen Ghasemi Varnamkhasti Influence of Oxygen Partial Pressure on Opto-Electrical Properties, Crystallite Size and Dislocation Density of Sn Doped In $_{2}$ 2 O $_{3}$ 3 Nanostructures, Journal of Electronic Materials, Volume 45 (2016) no. 10, p. 5395 | DOI:10.1007/s11664-016-4697-9
T.H. Simm; P.J. Withers; J. Quinta da Fonseca An evaluation of diffraction peak profile analysis (DPPA) methods to study plastically deformed metals, Materials Design, Volume 111 (2016), p. 331 | DOI:10.1016/j.matdes.2016.08.091
A. Harte; T. Seymour; E.M. Francis; P. Frankel; S.P. Thompson; D. Jädernäs; J. Romero; L. Hallstadius; M. Preuss Advances in synchrotron x-ray diffraction and transmission electron microscopy techniques for the investigation of microstructure evolution in proton- and neutron-irradiated zirconium alloys, Journal of Materials Research, Volume 30 (2015) no. 9, p. 1349 | DOI:10.1557/jmr.2015.65
Yanzhi Zhang; Xinjian Zhang; Xianglin Chen; Guan Weijun; Xiaolin Wang Effect of grain size on phase stability of monoclinic U–Nb alloy during low-temperature aging, Journal of Nuclear Materials, Volume 465 (2015), p. 167 | DOI:10.1016/j.jnucmat.2015.05.020
V. Soleimanian; S.R. Aghdaee X-ray diffraction analysis of the effect of annealing temperature on the microstructure of magnesium oxide nanopowder, Journal of Physics and Chemistry of Solids, Volume 81 (2015), p. 1 | DOI:10.1016/j.jpcs.2014.12.020
Z. Chen; J. Li; A. Borbely; G. Ji; S.Y. Zhong; Y. Wu; M.L. Wang; H.W. Wang The effects of nanosized particles on microstructural evolution of an in-situ TiB2/6063Al composite produced by friction stir processing, Materials Design, Volume 88 (2015), p. 999 | DOI:10.1016/j.matdes.2015.09.127
Y. Tang; Z. Chen; A. Borbély; G. Ji; S.Y. Zhong; D. Schryvers; V. Ji; H.W. Wang Quantitative study of particle size distribution in an in-situ grown Al–TiB2 composite by synchrotron X-ray diffraction and electron microscopy, Materials Characterization, Volume 102 (2015), p. 131 | DOI:10.1016/j.matchar.2015.03.003
A. Wauthier-Monnin; T. Chauveau; O. Castelnau; H. Réglé; B. Bacroix The evolution with strain of the stored energy in different texture components of cold-rolled IF steel revealed by high resolution X-ray diffraction, Materials Characterization, Volume 104 (2015), p. 31 | DOI:10.1016/j.matchar.2015.04.005
Peng Fu; Chuanhai Jiang; Xueyan Wu; Zhongquan Zhang Surface Modification of 304 Steel Using Triple-Step Shot Peening, Materials and Manufacturing Processes, Volume 30 (2015) no. 6, p. 693 | DOI:10.1080/10426914.2015.1004702
M. Mojtahedi; M. Goodarzi; M. R. Aboutalebi; V. Soleimanian An investigation on the microstructure and defects in the mechanically milled Cu and Fe powders, Powder Diffraction, Volume 30 (2015) no. 1, p. 14 | DOI:10.1017/s0885715614000761
Flavien Vucko; Cédric Bosch; David Delafosse Experimental investigations of internal and effective stresses during fatigue loading of high-strength steel, Materials Science and Engineering: A, Volume 597 (2014), p. 381 | DOI:10.1016/j.msea.2014.01.016

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